Structural-phase transformations in α-Ti under different types of deformation at room temperature

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Abstract

A study of the phase transformation in technically pure titanium under different types of deformation: high pressure and high pressure torsion (HPT). The set of modern methods of the study included microindentation, X-ray diffraction, transmission electron microscopy, as well as EXAFS spectroscopy in synchrotron radiation for detailed studying a local atomic structure of phases. The correlation between the phase transformation course and the deformation method has been found. It has been shown that in contrast to pressure without a shear component, the shear deformation under high pressure at room temperature contributes to the occurrence of a high-temperature β-phase with a local atomic order different from that in the initial phase.

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About the authors

N. A. Shurygina

Bardin Central Research Institute for Ferrous Metallurgy; Russian Technological University MIREA

Author for correspondence.
Email: shnadya@yandex.ru
Russian Federation, Moscow, 105005; Moscow, 119454

R. V. Sundeev

Russian Technological University MIREA

Email: shnadya@yandex.ru
Russian Federation, Moscow, 119454

A. V. Shalimova

Bardin Central Research Institute for Ferrous Metallurgy

Email: shnadya@yandex.ru
Russian Federation, Moscow, 105005

A. A. Veligzhanin

Kurchatov Complex for Theoretical and Experimental Physics, National Research Center “Kurchatov Institute”

Email: shnadya@yandex.ru
Russian Federation, Moscow, 123182

E. N. Blinova

Bardin Central Research Institute for Ferrous Metallurgy

Email: shnadya@yandex.ru
Russian Federation, Moscow, 105005

A. M. Glezer

Bardin Central Research Institute for Ferrous Metallurgy

Email: shnadya@yandex.ru
Russian Federation, Moscow, 105005

O. P. Chernogorova

Baikov Institute of Metallurgy and Materials Science, RAS

Email: shnadya@yandex.ru
Russian Federation, Moscow, 119334

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Supplementary files

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2. Fig. 1. Diffraction pattern of VT1-0 titanium samples in the initial state and after applying a pressure of 6 GPa for 10 min.

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3. Fig. 2. Electron microscopic images of the alloy microstructure in the initial state (a) and after applying a pressure of 6 GPa for 10 min (b).

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4. Fig. 3. Comparison of the experimental (transparent blue dots) and calculated EXAFS spectra (solid lines) in R-space for the VT1-0 sample in the initial state (a), after applying a pressure of 6 GPa with a holding time of 10 minutes (b), after HPT for 1 revolution (c), after HPT for 4 revolutions (d).

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