Morphology and Particle Size Distribution of Sulfonated Сarbon Black

O. A. Knyazheva; Княжева О. А.; O. A. Kokhanovskaya; Кохановская О. А.; M. V. Trenikhin; Тренихин М. В.; V. A. Drozdov; Дроздов В. А.; O. N. Baklanova; Бакланова О. Н.; A. B. Arbuzov; Арбузов А. Б.; A. V. Syrieva; Сырьева А. В.; N. N. Leont’eva; Леонтьева Н. Н.; A. V. Lavrenov; Лавренов А. В.

doi:10.31857/S0044185622600095

Morphology and Particle Size Distribution of Sulfonated Сarbon Black

Authors: Knyazheva O.A.¹, Kokhanovskaya O.A.¹, Trenikhin M.V.¹, Drozdov V.A.¹, Baklanova O.N.¹, Arbuzov A.B.¹, Syrieva A.V.¹, Leont’eva N.N.¹, Lavrenov A.V.¹
Affiliations:
1. Center of New Chemical Technologies BIC, Boreskov Institute of Catalysis, 644040, Omsk, Russia
Issue: Vol 59, No 1 (2023)
Pages: 64-72
Section: НАНОРАЗМЕРНЫЕ И НАНОСТРУКТУРИРОВАННЫЕ МАТЕРИАЛЫ И ПОКРЫТИЯ
URL: https://gynecology.orscience.ru/0044-1856/article/view/663843
DOI: https://doi.org/10.31857/S0044185622600095
EDN: https://elibrary.ru/PULNLM
ID: 663843

Cite item

Full Text

Open Access
Restricted Access

Access granted
Restricted Access

Subscription Access

Abstract
About the authors
References
Supplementary files
Statistics

Abstract

Modification of the surface of carbon black (CB) of the N326 is performed by treatment in an aqueous solution of sulfanilic acid with the addition of sodium nitrite. It is shown that the covalent modification of sulfonic groups in the amount of 0.25 up to 2.62 μmol/m2 on the carbon surface does not result in any substantial change in the specific surface area (84–85 m2/g) and dibutyl phthalate absorption number of the aggregates of carbon black (of 70–76 cm3/100 g). A sample of CB with the density of coating with sulfonic groups of 2.62 μmol/m2 is distinguished by the monomodal size distribution of carbon particles at an average diameter of about 250 nm and makes it possible to form highly stable aqueous suspensions.

Keywords

carbon black, sulfonation, particle size, aggregates, aqueous suspension

References

Min-Joo K., Young-Jung H., Fan-Long J., Soo-Jin P. // Carbon Lett. 2016. V. 18. P. 1–10.
Al-Ghamdi A.A., Al-Hartomy O.A., Al-Solamy F.R., Dishovskyc N., Malinova P., Atanasova G., Atanasov N. // Composites Part B. 2016. V. 96. P. 231–241.
Woonjung Kima, Jihyun Baea, Chul Hun Eumb, Jongjin Junga, Seungho Leea // Microchemical J. 2018. V. 142. P. 167–174.
Grulke E.A., Rice S.B., Xiong J.Ch., Yamamoto K., Yoon T.H., Thomson K., Saffaripour M., Smallwood G.J., Lambert J.W., Stromberg A.J., Macy R., Briot N.J., Qian D. // Carbon. 2018. V. 130. P. 822–833.
Lockwood F.C., Van Niekerk J.E. // Combust. Flame. 1995. V. 103. P. 76–90.
Medalia A.I. // J. Colloid Interface Sci. 1967. V. 24. P. 393–404.
Donnet, J.-B., Bansal R.G., Wang M.-J. Carbon Black: Science and Technology. J- 2nd RevisedEdition. N.Y., 1993.
Раздьяконова Г.И. // Каучук и резина. 2013. № 4. С. 36–39.
Гришин Б.С., Воронов В.С., Ельшевская Е.А., Сапронов В.А. // Каучук и резина. 1980. № 10. С. 24–27.
Nakajima N., Harrell E.R. // Rubb. Chem. Technol. 1983. V. 56. P. 197–209.
Topcir B. // Rubb. Age. 1973. V. 105. P. 25–33.
Speranza G. // Journal of Carbon Research. 2019. V. 5. P. 84.
Xinyu Yang, Zhaolun Wang, Mingchu Pan // Advanced Materials Research. 2011. V. 189–193. P. 3836.
Anton W.L., Wolfe M.S., Kluth A.W. // Patent WO2016100009A1. 2014.
Hideto Yamazaki // Patent JPH07331141A. 1994.
Nagasawa, Toshiyuki Yawata-shi, Kyoto-fu, Kihara, Tetsuji Takatsuki-shi, Osaka-fu, Itoh, Sohko Neyagawa-shi, Osaka-fu // EP 0 778 325 B1. 2001.
Buxbaum Gunter. Industrial inorganic pigments. Wiley-VCH, 1998. 307 p.
Adams C.E., Belmont J.A. // Patent 5707432 US. 1996.
Boehm H.P. // Carbon. 1994. V. 32. P. 759–769.
Bansal R.C., Goyal M. Activated carbon Adsorption. – Boca Raton: Taylor and Francis Group, 2005. 498 p.
Ishizaki C., Marti I. // Carbon. 1981. V. 19. P. 409–412.
Shin S., Jang J., Yoon S.-H., Mochida I. // Carbon. 1997. V. 35. P. 1739–1743.
Ying Zhao, Bo Sun, Yizhuang Xu, Dujin Wang, Shifu Weng, Jinguang Wu, Duanfu Xu, Guangxian Xu // Journal of Molecular Structure. 2001. V. 560. P. 115–120.
Оаэ С. Химия органических соединений серы / Пер. с япон. Бин Я.Ю., Нефедов Б.К. под ред. Прилежаевой Е.Н. М.: Химия, 1975. 512 с.